SOL-GEL PROCESSING OF PbTiO//3, PbZrO//3, PZT, AND PLZT THIN FILMS.

K. D. Budd, Sandwip Dey, D. A. Payne

Research output: Chapter in Book/Report/Conference proceedingConference contribution

677 Citations (Scopus)

Abstract

Thin films were fabricated in the PLZT system by spin casting solutions of complex alkoxides prepared by reacting Pb and La acetates with Zr and Ti alkoxides. Perovskite phases crystallized from bulk gels between 450 degree C-600 degree C depending on composition. Thin coatings of dilute solutions generally resulted in continuous crack-free layers, with good adhesion to silicon and fused silica substrate materials. Thicker films were prepared by multiple deposition techniques. The influence of hydrolysis water content and precursor reactivity on pyrolysis behavior, cracking tendency, and microstructure are discussed.

Original languageEnglish (US)
Title of host publicationBritish Ceramic Proceedings
EditorsB.C.H. Steele
Place of PublicationStoke-on-Trent, Engl
PublisherInst of Ceramics
Pages107-121
Number of pages15
Edition36
StatePublished - 1985
Externally publishedYes

Fingerprint

Thin films
Fused silica
Thick films
Perovskite
Water content
Hydrolysis
Casting
Pyrolysis
Adhesion
Gels
Cracks
Silicon
Coatings
Microstructure
Substrates
Chemical analysis

ASJC Scopus subject areas

  • Engineering(all)

Cite this

Budd, K. D., Dey, S., & Payne, D. A. (1985). SOL-GEL PROCESSING OF PbTiO//3, PbZrO//3, PZT, AND PLZT THIN FILMS. In B. C. H. Steele (Ed.), British Ceramic Proceedings (36 ed., pp. 107-121). Stoke-on-Trent, Engl: Inst of Ceramics.

SOL-GEL PROCESSING OF PbTiO//3, PbZrO//3, PZT, AND PLZT THIN FILMS. / Budd, K. D.; Dey, Sandwip; Payne, D. A.

British Ceramic Proceedings. ed. / B.C.H. Steele. 36. ed. Stoke-on-Trent, Engl : Inst of Ceramics, 1985. p. 107-121.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Budd, KD, Dey, S & Payne, DA 1985, SOL-GEL PROCESSING OF PbTiO//3, PbZrO//3, PZT, AND PLZT THIN FILMS. in BCH Steele (ed.), British Ceramic Proceedings. 36 edn, Inst of Ceramics, Stoke-on-Trent, Engl, pp. 107-121.
Budd KD, Dey S, Payne DA. SOL-GEL PROCESSING OF PbTiO//3, PbZrO//3, PZT, AND PLZT THIN FILMS. In Steele BCH, editor, British Ceramic Proceedings. 36 ed. Stoke-on-Trent, Engl: Inst of Ceramics. 1985. p. 107-121
Budd, K. D. ; Dey, Sandwip ; Payne, D. A. / SOL-GEL PROCESSING OF PbTiO//3, PbZrO//3, PZT, AND PLZT THIN FILMS. British Ceramic Proceedings. editor / B.C.H. Steele. 36. ed. Stoke-on-Trent, Engl : Inst of Ceramics, 1985. pp. 107-121
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