Optimizing the accuracy and precision of the single-pulse Laue technique for synchrotron photo-crystallography

Radosaw Kamiński, Timothy Graber, Jason B. Benedict, Robert Henning, Yu Sheng Chen, Stephan Scheins, Marc Messerschmidt, Philip Coppens

Research output: Contribution to journalArticle

8 Citations (Scopus)

Abstract

The accuracy that can be achieved in single-pulse pump-probe Laue experiments is discussed. It is shown that with careful tuning of the experimental conditions a reproducibility of the intensity ratios of equivalent intensities obtained in different measurements of 3-4% can be achieved. The single-pulse experiments maximize the time resolution that can be achieved and, unlike stroboscopic techniques in which the pump-probe cycle is rapidly repeated, minimize the temperature increase due to the laser exposure of the sample.

Original languageEnglish (US)
Pages (from-to)479-485
Number of pages7
JournalJournal of Synchrotron Radiation
Volume17
Issue number4
DOIs
StatePublished - Jul 2 2010
Externally publishedYes

Fingerprint

Crystallography
Synchrotrons
crystallography
synchrotrons
Pumps
pumps
probes
pulses
Tuning
Experiments
tuning
cycles
Lasers
lasers
Temperature
temperature

Keywords

  • accuracy
  • Laue method
  • photo-crystallography
  • RATIO method
  • single-pulse diffraction

ASJC Scopus subject areas

  • Instrumentation
  • Nuclear and High Energy Physics
  • Radiation

Cite this

Kamiński, R., Graber, T., Benedict, J. B., Henning, R., Chen, Y. S., Scheins, S., ... Coppens, P. (2010). Optimizing the accuracy and precision of the single-pulse Laue technique for synchrotron photo-crystallography. Journal of Synchrotron Radiation, 17(4), 479-485. https://doi.org/10.1107/S0909049510019710

Optimizing the accuracy and precision of the single-pulse Laue technique for synchrotron photo-crystallography. / Kamiński, Radosaw; Graber, Timothy; Benedict, Jason B.; Henning, Robert; Chen, Yu Sheng; Scheins, Stephan; Messerschmidt, Marc; Coppens, Philip.

In: Journal of Synchrotron Radiation, Vol. 17, No. 4, 02.07.2010, p. 479-485.

Research output: Contribution to journalArticle

Kamiński, Radosaw ; Graber, Timothy ; Benedict, Jason B. ; Henning, Robert ; Chen, Yu Sheng ; Scheins, Stephan ; Messerschmidt, Marc ; Coppens, Philip. / Optimizing the accuracy and precision of the single-pulse Laue technique for synchrotron photo-crystallography. In: Journal of Synchrotron Radiation. 2010 ; Vol. 17, No. 4. pp. 479-485.
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