Early detection of nanoparticle growth from x-ray reciprocal space mapping

Nadia Zatsepin, Ruben A. Dilanian, Andrei Y. Nikulin, Brian M. Gable, Barry C. Muddle, Osami Sakata

Research output: Contribution to journalArticle

5 Citations (Scopus)

Abstract

The potential for nondestructive in situ detection of the formation of weakly diffracting nanoparticles has been confirmed by a combination of experiment and simulation. A triple axis diffractometer was used to collect two-dimensional reciprocal space maps of diffracted synchrotron x-rays from nanoscale Al2 Cu precipitates embedded in a bulk metallic matrix. The appearance and asymmetric profile of the monochromator pseudostreaks are demonstrated to be indicative of the sensitivity of the technique to both the presence and orientation of the nanoparticles. This is a fundamental step toward in situ detection of sparsely dispersed, embedded nanoparticles and to quantitative temporal studies of particle number, scale, and dispersion.

Original languageEnglish (US)
Article number034101
JournalApplied Physics Letters
Volume92
Issue number3
DOIs
StatePublished - Feb 1 2008
Externally publishedYes

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nanoparticles
x rays
monochromators
diffractometers
precipitates
synchrotrons
sensitivity
matrices
profiles
simulation

ASJC Scopus subject areas

  • Physics and Astronomy (miscellaneous)

Cite this

Zatsepin, N., Dilanian, R. A., Nikulin, A. Y., Gable, B. M., Muddle, B. C., & Sakata, O. (2008). Early detection of nanoparticle growth from x-ray reciprocal space mapping. Applied Physics Letters, 92(3), [034101]. https://doi.org/10.1063/1.2829606

Early detection of nanoparticle growth from x-ray reciprocal space mapping. / Zatsepin, Nadia; Dilanian, Ruben A.; Nikulin, Andrei Y.; Gable, Brian M.; Muddle, Barry C.; Sakata, Osami.

In: Applied Physics Letters, Vol. 92, No. 3, 034101, 01.02.2008.

Research output: Contribution to journalArticle

Zatsepin, N, Dilanian, RA, Nikulin, AY, Gable, BM, Muddle, BC & Sakata, O 2008, 'Early detection of nanoparticle growth from x-ray reciprocal space mapping', Applied Physics Letters, vol. 92, no. 3, 034101. https://doi.org/10.1063/1.2829606
Zatsepin N, Dilanian RA, Nikulin AY, Gable BM, Muddle BC, Sakata O. Early detection of nanoparticle growth from x-ray reciprocal space mapping. Applied Physics Letters. 2008 Feb 1;92(3). 034101. https://doi.org/10.1063/1.2829606
Zatsepin, Nadia ; Dilanian, Ruben A. ; Nikulin, Andrei Y. ; Gable, Brian M. ; Muddle, Barry C. ; Sakata, Osami. / Early detection of nanoparticle growth from x-ray reciprocal space mapping. In: Applied Physics Letters. 2008 ; Vol. 92, No. 3.
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