3D microstructural characterization and mechanical properties of constituent particles in Al 7075 alloys using X-ray synchrotron tomography and nanoindentation

Sudhanshu S. Singh, Cary Schwartzstein, Jason J. Williams, Xianghui Xiao, Francesco De Carlo, Nikhilesh Chawla

Research output: Contribution to journalArticle

46 Citations (Scopus)

Abstract

Inclusions (constituent particles) in Al 7075 alloys can be classified as Fe-bearing and Si-bearing inclusions. They play important roles in the deformation behavior, particular under fatigue loading. Thus, in order to understand the deformation behavior under fatigue loading of Al 7075 alloys, it is important to investigate the size and distribution of these inclusions and porosity in the material, along with their mechanical properties. X-ray synchrotron tomography was used to obtain the 3D microstructure of these microconstituents in Al 7075 alloy. Quantitative analysis in terms of volume, size, and morphology of inclusions and porosity was performed. The mechanical properties of these constituent particles along with the matrix were obtained using nanoindentation. Scanning electron microscopy (SEM) and EDS was used to analyze the indentations after testing. The Young's modulus and hardness of all inclusions were higher than the matrix. The Young's modulus values of Al 7Cu2Fe, Al23Fe4Cu, and Mg 2Si were measured to be 160.2 ± 10.9, 139.5 ± 3.7, and 94.8 ± 7.5 GPa respectively. Values of hardness of Al7Cu 2Fe, Al23Fe4Cu, and Mg2Si were 8.8 ± 0.9, 7.5 ± 0.8, and 5.2 ± 0.5 GPa respectively. Comparison of these values with nanoindentation data in the literature was also conducted.

Original languageEnglish (US)
Pages (from-to)163-174
Number of pages12
JournalJournal of Alloys and Compounds
Volume602
DOIs
StatePublished - Jul 25 2014

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Nanoindentation
Synchrotrons
Tomography
X rays
Bearings (structural)
Mechanical properties
Porosity
Elastic moduli
Hardness
Fatigue of materials
Indentation
Energy dispersive spectroscopy
Microstructure
Scanning electron microscopy
Testing
Chemical analysis

Keywords

  • Mechanical properties
  • Microstructure
  • Multiphase intermetallics
  • Nanoindentation
  • X-ray tomography

ASJC Scopus subject areas

  • Mechanical Engineering
  • Mechanics of Materials
  • Materials Chemistry
  • Metals and Alloys

Cite this

3D microstructural characterization and mechanical properties of constituent particles in Al 7075 alloys using X-ray synchrotron tomography and nanoindentation. / Singh, Sudhanshu S.; Schwartzstein, Cary; Williams, Jason J.; Xiao, Xianghui; De Carlo, Francesco; Chawla, Nikhilesh.

In: Journal of Alloys and Compounds, Vol. 602, 25.07.2014, p. 163-174.

Research output: Contribution to journalArticle

Singh, Sudhanshu S. ; Schwartzstein, Cary ; Williams, Jason J. ; Xiao, Xianghui ; De Carlo, Francesco ; Chawla, Nikhilesh. / 3D microstructural characterization and mechanical properties of constituent particles in Al 7075 alloys using X-ray synchrotron tomography and nanoindentation. In: Journal of Alloys and Compounds. 2014 ; Vol. 602. pp. 163-174.
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