• 4139 Citations
  • 36 h-Index
1995 …2022
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Research Output 1995 2019

  • 4139 Citations
  • 36 h-Index
  • 128 Article
  • 5 Conference contribution
  • 1 Chapter
  • 1 Review article
2019

Chapter 18: NMR Characterization of Silk

Guo, C. & Yarger, J. L., Jan 1 2019, Optimizing NMR Methods for Structure Elucidation: Characterizing Natural Products and Other Organic Compounds. Sun, P., Zhang, R. & Miyoshi, T. (eds.). 20 ed. Royal Society of Chemistry, p. 420-456 37 p. (New Developments in NMR; vol. 2019-January, no. 20).

Research output: Chapter in Book/Report/Conference proceedingChapter

Silk
Nuclear magnetic resonance
Biocompatible Materials
Insects
Mechanical properties
Dicarboxylic Acids
Triazoles
dicarboxylic acids
Gold
Metal ions
1 Citation (Scopus)

Proton Transfer and Ionicity: An 15 N NMR Study of Pyridine Base Protonation

Hasani, M., Amin, S. A., Yarger, J., Davidowski, S. K. & Angell, C., Feb 28 2019, In : Journal of Physical Chemistry B. 123, 8, p. 1815-1821 7 p.

Research output: Contribution to journalArticle

Proton transfer
Protonation
Pyridine
Protons
pyridines
1 Citation (Scopus)
Open Access
Polyaniline
Gold
Raman scattering
Nanocomposites
Coloring Agents
2018
3 Citations (Scopus)

A New Version of the Lithium Ion Conducting Plastic Crystal Solid Electrolyte

Klein, I. S., Zhao, Z., Davidowski, S. K., Yarger, J. & Angell, C., Jan 1 2018, (Accepted/In press) In : Advanced Energy Materials.

Research output: Contribution to journalArticle

Solid electrolytes
Lithium
Electrolytes
Alkalies
Salts
6 Citations (Scopus)

Characterizing gold nanoparticles by NMR spectroscopy

Guo, C. & Yarger, J., Nov 1 2018, In : Magnetic Resonance in Chemistry. 56, 11, p. 1074-1082 9 p.

Research output: Contribution to journalArticle

Gold
Nuclear magnetic resonance spectroscopy
Nanoparticles
Surface chemistry
Size determination
9 Citations (Scopus)

Hierarchical spidroin micellar nanoparticles as the fundamental precursors of spider silks

Parent, L. R., Onofrei, D., Xu, D., Stengel, D., Roehling, J. D., Bennett Addison, J., Forman, C., Amin, S. A., Cherry, B., Yarger, J., Gianneschi, N. C. & Holland, G. P., Nov 6 2018, In : Proceedings of the National Academy of Sciences of the United States of America. 115, 45, p. 11507-11512 6 p.

Research output: Contribution to journalArticle

Spiders
Silk
Nanoparticles
Nanostructures
Micelles
5 Citations (Scopus)

Rapid Soft Tissue Approximation and Repair Using Laser-Activated Silk Nanosealants

Urie, R., Guo, C., Ghosh, D., Thelakkaden, M., Wong, V., Lee, J. K., Kilbourne, J., Yarger, J. & Rege, K., Jan 1 2018, (Accepted/In press) In : Advanced Functional Materials.

Research output: Contribution to journalArticle

silk
Silk
Repair
Tissue
Lasers
23 Citations (Scopus)

Structural Comparison of Various Silkworm Silks: An Insight into the Structure-Property Relationship

Guo, C., Zhang, J., Jordan, J. S., Wang, X., Henning, R. W. & Yarger, J., Jan 1 2018, In : Biomacromolecules. 19, 3, p. 906-917 12 p.

Research output: Contribution to journalArticle

Silk
Mechanical properties
Molecular structure
Fibers
Synchrotrons
32 Citations (Scopus)

Uncovering the structure-function relationship in spider silk

Yarger, J., Cherry, B. & Van Der Vaart, A., Mar 6 2018, In : Nature Reviews Materials. 3, 3, 8000.

Research output: Contribution to journalReview article

Silk
Fibers
Arthropod Proteins
Biopolymers
Synthetic fibers
2017
4 Citations (Scopus)

Highly Efficient Fumed Silica Nanoparticles for Peptide Bond Formation: Converting Alanine to Alanine Anhydride

Guo, C., Jordan, J. S., Yarger, J. & Holland, G. P., May 24 2017, In : ACS Applied Materials and Interfaces. 9, 20, p. 17653-17661 9 p.

Research output: Contribution to journalArticle

Anhydrides
Silicon Dioxide
Alanine
Peptides
Silica
3 Citations (Scopus)

Hydrogen mobility in the lightest reversible metal hydride, LiBeH3

Mamontov, E., Kolesnikov, A. I., Sampath, S. & Yarger, J., Dec 1 2017, In : Scientific Reports. 7, 1, 16244.

Research output: Contribution to journalArticle

metal hydrides
hydrogen
beryllium hydrides
lithium hydrides
sublattices
1 Citation (Scopus)

Silicon hydrogensulfates: Solid acids with exceptional 25 °c conductivities and possible electrochemical device applications

Klein, I. S., Davidowski, S. K., Yarger, J. & Angell, C., 2017, In : Journal of Materials Chemistry A. 5, 27, p. 14092-14100 9 p.

Research output: Contribution to journalArticle

Silicon
Electrolytes
Fuel cells
Acids
Protonation
4 Citations (Scopus)

Understanding iridium oxide nanoparticle surface sites by their interaction with catechol

Finkelstein-Shapiro, D., Fournier, M., Méndez-Hernández, D. D., Guo, C., Calatayud, M., Moore, T., Moore, A., Gust, D. & Yarger, J., 2017, In : Physical Chemistry Chemical Physics. 19, 24, p. 16151-16158 8 p.

Research output: Contribution to journalArticle

iridium
Nanoparticles
nanoparticles
oxides
Electrochemistry
2016
10 Citations (Scopus)

A flexible all-inorganic fuel cell membrane with conductivity above Nafion, and durable operation at 150 °c

Ansari, Y., Tucker, T. G., Huang, W., Klein, I. S., Lee, S. Y., Yarger, J. & Angell, C., Jan 30 2016, In : Journal of Power Sources. 303, p. 142-149 8 p.

Research output: Contribution to journalArticle

Cell membranes
fuel cells
Fuel cells
membranes
Membranes
7 Citations (Scopus)

A SAXS-WAXS study of the endothermic transitions in amorphous or supercooled liquid itraconazole

Benmore, C. J., Mou, Q., Benmore, K. J., Robinson, D. S., Neuefeind, J., Ilavsky, J., Byrn, S. R. & Yarger, J., Nov 20 2016, In : Thermochimica Acta. 644, p. 1-5 5 p.

Research output: Contribution to journalArticle

Itraconazole
Liquids
liquids
Neutron scattering
Scattering
5 Citations (Scopus)

Characterizing mixed phosphonic acid ligand capping on CdSe/ZnS quantum dots using ligand exchange and NMR spectroscopy

Davidowski, S. K., Lisowski, C. E. & Yarger, J., Mar 1 2016, In : Magnetic Resonance in Chemistry. 54, 3, p. 234-238 5 p.

Research output: Contribution to journalArticle

Nuclear magnetic resonance spectroscopy
Semiconductor quantum dots
Ligands
Acids
Phosphorous Acids
23 Citations (Scopus)

Direct Evidence of Chelated Geometry of Catechol on TiO2 by a Combined Solid-State NMR and DFT Study

Finkelstein-Shapiro, D., Davidowski, S. K., Lee, P. B., Guo, C., Holland, G. P., Rajh, T., Gray, K. A., Yarger, J. & Calatayud, M., Oct 20 2016, In : Journal of Physical Chemistry C. 120, 41, p. 23625-23630 6 p.

Research output: Contribution to journalArticle

Density functional theory
Nuclear magnetic resonance
density functional theory
solid state
nuclear magnetic resonance
2 Citations (Scopus)

Lysine-Capped Silica Nanoparticles: A Solid-State NMR Spectroscopy Study

Guo, C., Holland, G. P. & Yarger, J., Jan 1 2016, In : MRS Advances. 1, 31, p. 2261-2266 6 p.

Research output: Contribution to journalArticle

lysine
Silicon Dioxide
Nuclear magnetic resonance spectroscopy
Lysine
Silica
11 Citations (Scopus)

Microscale Mechanism of Age Dependent Wetting Properties of Prickly Pear Cacti (Opuntia)

Rykaczewski, K., Jordan, J. S., Linder, R., Woods, E. T., Sun, X., Kemme, N., Manning, K. C., Cherry, B., Yarger, J. & Majure, L. C., Sep 13 2016, In : Langmuir. 32, 36, p. 9335-9341 7 p.

Research output: Contribution to journalArticle

microbalances
wetting
Wetting
epidermis
Water
22 Citations (Scopus)

NMR Characterization of Ionicity and Transport Properties for a Series of Diethylmethylamine Based Protic Ionic Liquids

Davidowski, S. K., Thompson, F., Huang, W., Hasani, M., Amin, S. A., Angell, C. & Yarger, J., May 12 2016, In : Journal of Physical Chemistry B. 120, 18, p. 4279-4285 7 p.

Research output: Contribution to journalArticle

Ionic Liquids
Ionic liquids
Transport properties
transport properties
Nuclear magnetic resonance
15 Citations (Scopus)

On the Use of a Protic Ionic Liquid with a Novel Cation To Study Anion Basicity

Hasani, M., Yarger, J. & Angell, C., Sep 5 2016, In : Chemistry - A European Journal. 22, 37, p. 13312-13319 8 p.

Research output: Contribution to journalArticle

Ionic Liquids
Alkalinity
Ionic liquids
Anions
Cations
11 Citations (Scopus)

Secondary structure adopted by the Gly-Gly-X repetitive regions of dragline spider silk

Gray, G. M., van der Vaart, A., Guo, C., Jones, J., Onofrei, D., Cherry, B., Lewis, R. V., Yarger, J. & Holland, G. P., Dec 2 2016, In : International Journal of Molecular Sciences. 17, 12, 2023.

Research output: Contribution to journalArticle

spiders
silk
Spiders
Silk
Nucleic Acid Repetitive Sequences

Structure and properties in synthetic MSUM and the corresponding biomaterial

Brune, A. B., Holland, G. P., Yarger, J. & Petuskey, W., Jan 1 2016, In : MRS Advances. 1, 36, p. 2551-2556 6 p.

Research output: Contribution to journalArticle

Biocompatible Materials
Biomaterials
Needles
Biomimetic materials
Nuclear magnetic resonance
17 Citations (Scopus)

Surface and wetting properties of embiopteran (webspinner) nanofiber silk

Popp, T. M. O., Addison, J. B., Jordan, J. S., Damle, V. G., Rykaczewski, K., Chang, L-Y., Stokes, G. Y., Edgerly, J. S. & Yarger, J., 2016, In : Langmuir. 32, 18, p. 4681-4687 7 p.

Research output: Contribution to journalArticle

silk
Silk
Nanofibers
surface properties
wetting
5 Citations (Scopus)

Using containerless methods to develop amorphous pharmaceuticals

Weber, J. K. R., Benmore, C. J., Suthar, K. J., Tamalonis, A. J., Alderman, O. L. G., Sendelbach, S., Kondev, V., Yarger, J., Rey, C. A. & Byrn, S. R., Jan 25 2016, (Accepted/In press) In : Biochimica et Biophysica Acta - General Subjects.

Research output: Contribution to journalArticle

Pharmaceutical Preparations
Spray drying
Acoustics
Solubility
Processing
2015
5 Citations (Scopus)

Enhanced electrochemical performance of LiFe<inf>0.4</inf>Mn<inf>0.6</inf>(PO<inf>4</inf>)<inf>1 - x</inf>(BO<inf>3</inf>)<inf>x</inf> as cathode material for lithium ion batteries

Sin, B. C., Singh, L., Lee, K. E., Kim, M., Cho, M., Yarger, J., Woo, S. K., Lee, H. I. & Lee, Y., Nov 1 2015, In : Journal of Electroanalytical Chemistry. 756, p. 50-60 11 p., 2236.

Research output: Contribution to journalArticle

Phosphates
Cathodes
Boron
Ball mills
Electron energy loss spectroscopy
12 Citations (Scopus)

Gold nanoparticle-doped silk film as biocompatible SERS substrate

Guo, C., Hall, G. N., Addison, J. B. & Yarger, J., 2015, In : RSC Advances. 5, 3, p. 1937-1942 6 p.

Research output: Contribution to journalArticle

Silk
Gold
Nanoparticles
Substrates
Trace analysis
21 Citations (Scopus)

Molecular Dynamics of Spider Dragline Silk Fiber Investigated by 2H MAS NMR

Shi, X., Holland, G. P. & Yarger, J., Mar 9 2015, In : Biomacromolecules. 16, 3, p. 852-859 8 p.

Research output: Contribution to journalArticle

Magic angle spinning
Silk
Molecular dynamics
Nuclear magnetic resonance
Fibers
4 Citations (Scopus)

Protein secondary structure of Green Lynx spider dragline silk investigated by solid-state NMR and X-ray diffraction

Xu, D., Shi, X., Thompson, F., Weber, W. S., Mou, Q. & Yarger, J., Nov 1 2015, In : International Journal of Biological Macromolecules. 81, p. 171-179 9 p.

Research output: Contribution to journalArticle

Lynx
Secondary Protein Structure
Nanocrystallites
Spiders
Silk
17 Citations (Scopus)

Type I Clathrates as Novel Silicon Anodes: An Electrochemical and Structural Investigation

Li, Y., Raghavan, R., Wagner, N. A., Davidowski, S. K., Baggetto, L., Zhao, R., Cheng, Q., Yarger, J., Veith, G. M., Ellis-Terrell, C., Miller, M. A., Chan, K. S. & Chan, C., 2015, In : Advanced Science. 2, 6, 1500057.

Research output: Contribution to journalArticle

clathrates
Silicon
Anodes
Electrodes
anodes
4 Citations (Scopus)
X ray scattering
X-Rays
X rays
MATLAB
Molecular Structure
2014
7 Citations (Scopus)

Adsorption and release of surfactant into and from multifunctional zwitterionic poly(NIPAm-co-DMAPMA-co-AAc) microgel particles

Chen, H., Kelley, M., Guo, C., Yarger, J. & Dai, L., Nov 3 2014, (Accepted/In press) In : Journal of Colloid and Interface Science.

Research output: Contribution to journalArticle

Nonionic surfactants
Dispersions
Surface-Active Agents
Swelling
Polymers
34 Citations (Scopus)

Effects of different post-spin stretching conditions on the mechanical properties of synthetic spider silk fibers

Albertson, A. E., Teulé, F., Weber, W., Yarger, J. & Lewis, R. V., Jan 2014, In : Journal of the Mechanical Behavior of Biomedical Materials. 29, p. 225-234 10 p.

Research output: Contribution to journalArticle

Silk
Stretching
Mechanical properties
Fibers
Proteins
11 Citations (Scopus)

Elucidating proline dynamics in spider dragline silk fibre using <sup>2</sup>H-<sup>13</sup>C HETCOR MAS NMR

Shi, X., Yarger, J. & Holland, G. P., May 14 2014, In : Chemical Communications. 50, 37, p. 4856-4859 4 p.

Research output: Contribution to journalArticle

Spiders
Silk
Proline
Nuclear magnetic resonance
Fibers
10 Citations (Scopus)

Exploring the backbone dynamics of native spider silk proteins in Black Widow silk glands with solution-state NMR spectroscopy

Xu, D., Yarger, J. & Holland, G. P., Aug 5 2014, In : Polymer (United Kingdom). 55, 16, p. 3879-3885 7 p.

Research output: Contribution to journalArticle

Silk
Nuclear magnetic resonance spectroscopy
Proteins
Biopolymers
Fibers
33 Citations (Scopus)

Mechanical and physical properties of recombinant spider silk films using organic and aqueous solvents

Tucker, C. L., Jones, J. A., Bringhurst, H. N., Copeland, C. G., Addison, J. B., Weber, W. S., Mou, Q., Yarger, J. & Lewis, R. V., Aug 11 2014, In : Biomacromolecules. 15, 8, p. 3158-3170 13 p.

Research output: Contribution to journalArticle

Silk
Physical properties
Mechanical properties
Water
Glutaral
9 Citations (Scopus)

Probing the nature of charge transfer at nano-bio interfaces: Peptides on metal oxide nanoparticles

Pilarisetty, T., Palma, J. L., Holland, G. P., Fromme, P., Yarger, J. & Mujica, V., Oct 16 2014, In : Journal of Physical Chemistry Letters. 5, 20, p. 3555-3559 5 p.

Research output: Contribution to journalArticle

Oxides
Peptides
peptides
metal oxides
Photosystem I Protein Complex
17 Citations (Scopus)

Reversible assembly of β-sheet nanocrystals within caddisfly silk

Addison, J. B., Weber, W. S., Mou, Q., Ashton, N. N., Stewart, R. J., Holland, G. P. & Yarger, J., Apr 14 2014, In : Biomacromolecules. 15, 4, p. 1269-1275 7 p.

Research output: Contribution to journalArticle

Silk
Nanocrystals
Ethylenediaminetetraacetic acid
Edetic Acid
Chelation

Reversible elastic deformation of functionalized sp2 carbon at pressures of up to 33 GPa

Soignard, E., Hochheimer, H. D., Yarger, J. & Raj, R., Oct 6 2014, In : Applied Physics Letters. 105, 14, 141901.

Research output: Contribution to journalArticle

elastic deformation
carbon
unloading
silicon
anvils
11 Citations (Scopus)

Structural characterization of nanofiber silk produced by embiopterans (webspinners)

Addison, J. B., Osborn Popp, T. M., Weber, W. S., Edgerly, J. S., Holland, G. P. & Yarger, J., 2014, In : RSC Advances. 40, 78, p. 41301-41313 13 p.

Research output: Contribution to journalArticle

Silk
Nanofibers
Nuclear magnetic resonance
Fibers
Alkanes
11 Citations (Scopus)

Structural hysteresis in dragline spider silks induced by supercontraction: An X-ray fiber micro-diffraction study

Sampath, S. & Yarger, J., 2014, In : RSC Advances. 5, 2, p. 1462-1473 12 p.

Research output: Contribution to journalArticle

Silk
Hysteresis
Regain
Diffraction
X rays
2013
11 Citations (Scopus)

2H-13C HETCOR MAS NMR for indirect detection of 2H quadrupole patterns and spin-Lattice relaxation rates

Shi, X., Yarger, J. & Holland, G. P., Jan 2013, In : Journal of Magnetic Resonance. 226, p. 1-12 12 p.

Research output: Contribution to journalArticle

Spin-lattice relaxation
Deuterium
spin-lattice relaxation
deuterium
quadrupoles
Spin-lattice relaxation
Deuterium
spin-lattice relaxation
deuterium
quadrupoles
6 Citations (Scopus)

Amino acid analysis of spider dragline silk using 1H NMR

Shi, X., Holland, G. P. & Yarger, J., 2013, In : Analytical Biochemistry. 440, 2, p. 150-157 8 p.

Research output: Contribution to journalArticle

Spiders
Silk
Magnetic Resonance Spectroscopy
Nuclear magnetic resonance
Amino Acids
10 Citations (Scopus)

A neutron-X-ray, NMR and calorimetric study of glassy Probucol synthesized using containerless techniques

Weber, J. K. R., Benmore, C. J., Tailor, A. N., Tumber, S. K., Neuefeind, J., Cherry, B., Yarger, J., Mou, Q., Weber, W. & Byrn, S. R., 2013, In : Chemical Physics. 424, p. 89-92 4 p.

Research output: Contribution to journalArticle

Probucol
Neutrons
Nuclear magnetic resonance
neutrons
X rays
39 Citations (Scopus)

Characterizing the secondary protein structure of black widow dragline silk using solid-state NMR and X-ray diffraction

Jenkins, J. E., Sampath, S., Butler, E., Kim, J., Henning, R. W., Holland, G. P. & Yarger, J., Oct 14 2013, In : Biomacromolecules. 14, 10, p. 3472-3483 12 p.

Research output: Contribution to journalArticle

Secondary Protein Structure
Silk
X-Ray Diffraction
Amino acids
Black Widow Spider
14 Citations (Scopus)

Determining hydrogen-bond interactions in spider silk with 1H-13C HETCOR fast MAS solid-state NMR and DFT proton chemical shift calculations

Holland, G. P., Mou, Q. & Yarger, J., Jul 28 2013, In : Chemical Communications. 49, 59, p. 6680-6682 3 p.

Research output: Contribution to journalArticle

Magic angle spinning
Silk
Chemical shift
Density functional theory
Protons
42 Citations (Scopus)

Elucidating silk structure using solid-state NMR

Asakura, T., Suzuki, Y., Nakazawa, Y., Holland, G. P. & Yarger, J., Dec 28 2013, In : Soft Matter. 9, 48, p. 11440-11450 11 p.

Research output: Contribution to journalArticle

silk
Silk
Nuclear magnetic resonance
solid state
nuclear magnetic resonance
2 Citations (Scopus)
Permittivity
Nuclear magnetic resonance
permittivity
tubes
Glass